Tricarbonylchlorido(6′,7′-dihydro-5′H-spiro[cyclopentane- 1,6′-dipyrido[3,2-d:2′,3′-f][1,3]diazepine] -κ2 N 1,N 11)rhenium(I)

O.R. Clegg, L.P. Harding, J.W. Miller, C.R. Rice

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)


In the title compound, [ReCl(C15H16N4)(CO)3], the ReI ion is coordinated in a distorted octa­hedral geometry by one Cl atom, two N atoms of the bidentate ligand and three carbonyl groups. The cyclo­pentane group is orientated in a transoid fashion with respect to the chloride ligand. The dihedral angle between the pryridine rings is 10.91 (12)°. In the crystal, N—H⋯Cl hydrogen bonds link complex mol­ecules, forming a two-dimensional network parallel to (001).
Original languageEnglish
Pages (from-to)m526
JournalActa Crystallographica Section E: Structure Reports Online
Issue number10
Publication statusPublished - Oct 2013


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